| Patrick Mills recently
joined the faculty at TAMUK in January
2006 as the Frank H. Dotterweich Chair
and Professor in the Department of Chemical
and Natural Gas Engineering. Before this
appointment, he was a Senior Research
Associate in the DuPont Company's Central
Research and Development Department in
Wilmington, Delaware where he was a member
of the Chemical Science and Engineering
Laboratory. During his 15+ years at DuPont,
he used his research and development expertise
in reaction kinetics, multiphase reaction
engineering, transport phenomena, and
experimental systems engineering to impact
many technology areas in various DuPont
businesses, such as Dacron, Nylon, Lycra,
White Pigments, Fluoroproducts, and Nonwovens.
In 1994, Dr. Mills developed the first
successful research collaboration with
the National Chemical Laboratory in Pune,
India. These efforts served as a prototype
that is now continuing through the former
DuPont Invista group in the UK. He was
also awarded an Engineering Excellence
Award from DuPont in 1996 for development
of the MARS system, which was an automated
catalyst testing productivity device.
Before joining the DuPont Company, Dr.
Mills worked for 10 years at the Monsanto
Corporate Research Center at the World
Headquarters in St. Louis and also at
the GE Corporate R&D Center in Schenectady,
New York. His research here utilized reaction
engineering for the discovery and development
of new molecules and processes in various
businesses and technologies, such as agricultural
and rubber chemicals, detergent hydrophobes,
aromatic polycarbonates, functionalized
olefinic polymers, and supercritical fluid
chromatographic separations. He also served
as a Research Associate Professor at Washington
University in St. Louis from 1988 to 1990.
In this capacity, he served as member
of the business and technology team that
commercialized the TAP® (Temporal
Analysis of Products) reactor system,
which is an experimental system used by
various university groups and companies
worldwide for the study of heterogeneous
catalyzed reactions. He also held appointments
as Adjunct Professor of Chemical and Natural Gas Engineering
at the University of Delaware and Washington
University in St. Louis where he taught
graduate courses in reaction engineering
and applied mathematics. Dr. Mills is
the author or co-author of over 110 publications
in Chemical and Natural Gas Engineering and applied mathematics,
has presented more than 125 papers at
professional society meetings, and is
named co-inventor on 2 patents.
Research Areas and Interests
Reaction engineering for multiphase catalytic
systems, polymerization reaction engineering,
pilot plant design and reactor scale-up
methods, micro-scale reactors and miniaturized
process plant systems, high-throughput
and parallel reactor systems, process
safety management, on-line process analytical
and on-line sensor systems, imaging science
in multiphase flow systems, tracer methods
in reaction engineering, heterogeneous
and homogeneous catalysis, applied mathematics
for reaction-transport systems.
Teaching Interests
- Reaction engineering for multiphase
catalyzed systems
- Special topics in reaction engineering-
Polymerization, bio-systems, and environmental
systems
- Continuing education short courses in
reaction engineering – introduction
to reaction engineering, multiphase reactors,
laboratory-scale reactors.
- Applied mathematics for scientists and
engineers
- Product engineering – science
and technology
Professional Experience
- Texas A&M University-Kingsville,
Kingsville, TX (2006 - Present)
- Chair, Frank H. Dotterweich
Frank H. Dotterweich College of Engineering
- Professor, Department
of Chemical and Natural Gas Engineering
- Senior Research Associate, DuPont Company's
Central Research and Development Department
in Wilmington, Delaware (1991– 2006)
- Senior Research Associate, Monsanto
Corporate Research Center, St. Louis
- Senior Research Associate,GE Corporate
R&D Center, Schenectady, New York
- Research Associate Professor at Washington
University in St. Louis (1988– 1990)
- Adjunct Professor of Chemical and Natural Gas Engineering,
University of Delaware, Delaware
- Adjunct Professor of Chemical and Natural Gas Engineering,
Washington University in St. Louis
Examples of Research Projects
and Process Technology Areas
- Fan Jet and Visualization Technologies
for Novel Nonwoven Processes - Novel Melt-Spun Elastomers for Lycra®
Spandex Fibers - Alternates Routes to Tetrahydrofuran
Monomer - Heterogeneous Catalysis Combinatorial
Research – Novel Tools and Applications
- Butane Oxidation VPO Catalyst Development
for the Asturias Riser - para-xylene Oxdidation Catalyst Improvement
and Multi-Stage Pilot Plant Process - Cyclohexane Oxidation Process Debottlenecking
- Polymer Functionalization by Catalytic
Hydroformylation - Tertiary-Butylamine and 4-Aminodiphenylamine
Catalysis - Novel Detergent Hydrophobes by an Oxo-Aldol
Process
- 2-Step Route to Ethylene Glycol by Hydroformylation
of Formaldehyde
Selected Publications
- P. L. Mills and J. F. Nicole, "Multiple
Automated Reactor System (MARS) - 1. A
Novel Reactor System for Detailed Testing
of Gas-Phase Heterogeneous Oxidation Catalysts,"
Industrial & Engineering Chemistry
Research, 44(16), 6435-6452 (2005).
- P. L. Mills and J. F. Nicole, "Multiple
Automated Reactor System (MARS) - 2. Effect
of Microreactor Configurations on Homogeneous
and Wall-Catalyzed Reactions for 1,3-Butadiene
Oxidation," Industrial & Engineering
Chemistry Research, 44(16), 6453-6465
(2005).
- R. V. Chaudhari and P. L. Mills, “Multiphase
Catalysis and Reaction Engineering for
Emerging Pharmaceutical Processes, Chemical and Natural Gas Engineering Science, 59(22/23), pp.5337
- 5344 (2004).
- P. L. Mills and J. F. Nicole, “A
Novel Reactor for High-Throughput Screening
of Gas-Solid Catalyzed Reactions,”
Chemical and Natural Gas Engineering Science 59(22/23),
pp.5337 - 5344 (2004).
- M. P. Dudukovic, F. Larachi, and P.
L. Mills, "Multiphase Reactors -
Current Knowledge & Future Trends,”
Catalysis Reviews - Science and Engineering,
44(1), pp 123-246 (2002).
- D. J. Quiram, K. F. Jensen, M. A. Schmidt,
J. F. Ryley, P. L. Mills, M. D. Wetzel,
J. A. Ashmead, R. D. Bryson, T. M. Delaney,
D. J. Kraus, and J. S. McCracken, “Development
of a Turnkey Multiple Microreactor Test
Station,” Proceedings of the 4th
International Conference on Microreaction
Technology (I. Rinard, ed.), pp. 55-61,
AIChE Press, New York, NY (2000).
- P. L. Mills, J. R. Turner, P. A. Ramachandran
and M. P. Dudukovic, “The Fischer-Tropsch
Synthesis in Slurry Bubble Column Reactors:
Analysis of Reactor Performance Using
the Axial Dispersion Model,” Chapter
5 in Three-Phase Sparged Reactors (K.
D. P. Nigam and A. Schumpe, eds.), pp.
339 - 386, Gordon and Breach, Amsterdam,
1996.
Selected Presentations
- P. L. Mills, "Current Status and
Future Directions on Laboratory-Scale
Multiphase Reactors," Plenary Lecture,
5th International Symposium on Catalysis
in Multiphase Reactors & 4th International
Symposium on Multifunctional Reactors,
Portoro-Portorose, Slovenia, June
15, 2005.
- R. V. Chaudhari and P. L. Mills, "Multiphase
Catalysis and Reaction Engineering for
Emerging Pharmaceutical Processes, The
18th International Symposium on Chemical
Reaction Engineering (ISCRE 18), Session
15: Multiphase Reactors, incl. Pharmaceutical
Reactions A., Chicago, IL, June 8, 2004.
- P. L. Mills and J. F. Nicole, "A
Novel Reactor for HTS of Gas-Solid Catalyzed
Reactions," The 18th International
Symposium on Chemical Reaction Engineering
(ISCRE 18), Session 15: Multiphase Reactors,
incl. Pharmaceutical Reactions A., Chicago,
IL, June 8, 2004.
- P. L. Mills, L. E. Manzer, and S. D.
Roy, “Green Chemistry Process Alternatives
for THF Manufacture,” Paper 551f,
AIChE 2003 Annual Meeting, Session 551
on Green Chemistry and Reaction Engineering
– III, San Francisco, CA, November
18, 2003.
- D. J. Quiram, P. L. Mills, J. F. Ryley,
M. D. Wetzel, J. W. Ashmead, R. D. Bryson,
D. J. Kraus, R. E. Mitchell, M. A. Schmidt,
and K. F. Jensen, “Construction
and Performance Evaluation of a Parallel
Microreactor System,” Paper 148e,
AIChE 2003 Annual Meeting, Session 148
on Pilot Plants: The Uniqueness of Small
Scale, San Francisco, CA, November 17,
2003.
- P. L. Mills, “Single and Multi-staged
Pilot Plants for the Oxidation of para-Xylene
to Terephthalic Acid,” Paper 149a,
AIChE 2003 Annual Meeting, Session 149
on Traditional and Novel Pilot Plant Reactors,
San Francisco, CA, November 18, 2003.
- P. L. Mills, "Current Status and
Future Directions in Lab-Scale Multiphase
Reactors," Paper 113, E. V. Murphree
Award Symposium in honor of Leo E. Manzer,
225th ACS Meeting, New Orleans, March
25, 2003.
Professional Affiliations
- Member, American Institute of Chemical
Engineers (AIChE)
- First Vice-Chair - AIChE Catalysis and
Reaction Engineering Division 20
- Member, Society for Industrial and Applied
Mathematics (SIAM)
- Member, Sigma Xi
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